4-Nitrobenzenesulfonyl chloride → N-[2-[bis(1-methylethyl)amino]ethyl]-4-nitrobenzene sulfonamide

HRID 255684

反応式

HRID 255684 の反応式
[N+:1]([C:4]1[CH:9]=[CH:8][C:7]([S:10](Cl)(=[O:12])=[O:11])=[CH:6][CH:5]=1)([O-:3])=[O:2].[CH:14]([N:17]([CH:21]([CH3:23])[CH3:22])[CH2:18][CH2:19][NH2:20])([CH3:16])[CH3:15]>>[CH3:15][CH:14]([N:17]([CH:21]([CH3:23])[CH3:22])[CH2:18][CH2:19][NH:20][S:10]([C:7]1[CH:8]=[CH:9][C:4]([N+:1]([O-:3])=[O:2])=[CH:5][CH:6]=1)(=[O:12])=[O:11])[CH3:16]

参加物

3

反応物 2

HCID 74044-Nitrobenzenesulfonyl chlorideHCID 84591,2-Ethanediamine, N1,N1-bis(1-methylethyl)-

生成物 1

HCID 13913719N-[2-[bis(1-methylethyl)amino]ethyl]-4-nitrobenzene sulfonamide

実験手順

p-Nitrobenzenesulfonyl chloride was reacted with N,N-diisopropyl ethylene diamine to give N-[2-[bis(1-methylethyl)amino]ethyl]-4-nitrobenzene sulfonamide as the free base, m.r. 86°-88° C.

出典と根拠

ORDレコード
ord-4f296ff22b9348ed943faa840eabd86b
出典データセット
uspto-grants-1987_10
特許番号
US04698445

関連ノート

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