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Trifluoroacetic acid → HCID 178464450、化合物
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Trifluoroacetic acid | HCID 6422 | — |
| 反応物 | 2-(Ethylamino)ethanol | HCID 8072 | — |
| 反応物 | 4-(Trifluoromethyl)phenyl carbonochloridate | HCID 15917597 | — |
| 反応物 | HCID 178484796 | HCID 178484796 | — |
| 生成物 | HCID 178464450 | HCID 178464450 | — |
反応手順
In analogy to examples 29.10 and 29.11, trans-Methansulfonic acid 5-(4-methyl amino-cyclohexyl)-pentyl ester.trifluoroacetic acid salt and 4-trifluoromethyl-phenyl chloroformate were reacted, followed by treatment with 2-ethylamino-ethanol to yield trans-(4-{5-[Ethyl-(2-hydroxy-ethyl)-amino]-pentyl}-cyclohexyl)-methyl-carbamic acid 4-trifluoromethyl-phenyl ester, MS: 459 (MH+).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US06858651B2 |
| 出典データセット | uspto-grants-2005_02 |
| ORD ID | ord-f2334a93a3a0489792031f1466a1defd |
| 出典メモ | uspto-grants-2005_02 |