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Trifluoroacetic acid → HCID 178483441、化合物
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Trifluoroacetic acid | HCID 6422 | — |
| 反応物 | 4-Chlorophenyl chloroformate | HCID 139059 | — |
| 反応物 | N-Methylcyclopropanamine | HCID 11029756 | — |
| 反応物 | HCID 178484796 | HCID 178484796 | — |
| 生成物 | HCID 178483441 | HCID 178483441 | — |
反応手順
In analogy to examples 29.10 and 29.11, trans-Methansulfonic acid 5-(4-methyl amino-cyclohexyl)-pentyl ester.trifluoroacetic acid salt and 4-chlorophenyl chloroformate were reacted, followed by treatment with N-methyl-N-cyclopropyl-amine to give trans {4-[5-(Cyclopropyl-methyl-amino)-pentyl]-cyclohexyl}-methyl-carbamic acid 4-chloro-phenyl ester, MS: 407 (MH+, 1Cl).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US06858651B2 |
| 出典データセット | uspto-grants-2005_02 |
| ORD ID | ord-6875583bff6945e984fb5976f86e7f0e |
| 出典メモ | uspto-grants-2005_02 |