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1-Chloroanthraquinone → Anthrimide
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 1-Chloroanthraquinone | HCID 6709 | — |
| 反応物 | Sodium Carbonate | HCID 10340 | — |
| 反応物 | Disperse Violet 1 | HCID 31420 | — |
| 触媒 | Cuprous chloride | HCID 62652 | — |
| 溶媒 | Nitrobenzene | HCID 7416 | — |
| 生成物 | Anthrimide | HCID 6700 | — |
反応手順
Following the procedure as descrilbed in Example 1, but suspending the 1-chloroanthraquinone, 1,4-diaminoanthraquinone, sodium carbonate and CuCl in 300 ml of nitrobenzene, the anthrimide is obtained in a yield corresponding to that of Example 1. When following a conventional procedure, i.e. mixing the components and heating them slowly, if such a concentrated reaction mixture is employed, the reaction can no longer be carried out in an agitator vessel.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04701281 |
| 出典データセット | uspto-grants-1987_10 |
| ORD ID | ord-a3d0b1a6bb41422fb40fef4e3f3f4b93 |
| 出典メモ | uspto-grants-1987_10 |