化工社化工社 化学情報印刷レポート · 研究参考用
Sulfuric Acid → Catechol
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Sulfuric Acid | HCID 1118 | — |
| 反応物 | Arsenic | HCID 5359596 | — |
| 反応物 | n-Hexylpyrocatechol | HCID 19900938 | — |
| 触媒 | Copper | HCID 23978 | — |
| 生成物 | Catechol | HCID 289 | — |
| 生成物 | 1-Hexene | HCID 11597 | — |
反応手順
100 ml of an aqueous solution containing sulfuric acid (200 g/l), copper (45 g/l) and arsenic (5.9 g/l) were poured into a 250 ml separatory funnel. Then a 0.3M solution of n-hexylpyrocatechol (100 ml), (a mixture of the two position isomers obtained from the reaction of 1-hexene with excess of pyrocatechol), was added into ESCAID 100; the mixture was strongly stirred for 10' and made then to settle for 30'.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04701311 |
| 出典データセット | uspto-grants-1987_10 |
| ORD ID | ord-7f93ba93cc1a4198905453e2317ded0e |
| 出典メモ | uspto-grants-1987_10 |