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HRID 256136作成日:2026年10月24日

Sulfuric Acid → Catechol

https://huagongshe.com/ja/reaction/256136

反応式

関与物質

役割名称HCID仕込み量
反応物Sulfuric AcidHCID 1118—
反応物ArsenicHCID 5359596—
反応物n-HexylpyrocatecholHCID 19900938—
触媒CopperHCID 23978—
生成物CatecholHCID 289—
生成物1-HexeneHCID 11597—

反応手順

100 ml of an aqueous solution containing sulfuric acid (200 g/l), copper (45 g/l) and arsenic (5.9 g/l) were poured into a 250 ml separatory funnel. Then a 0.3M solution of n-hexylpyrocatechol (100 ml), (a mixture of the two position isomers obtained from the reaction of 1-hexene with excess of pyrocatechol), was added into ESCAID 100; the mixture was strongly stirred for 10' and made then to settle for 30'.

情報源と証拠

DOI10.6084/m9.figshare.5104873.v1
特許番号US04701311
出典データセットuspto-grants-1987_10
ORD IDord-7f93ba93cc1a4198905453e2317ded0e
出典メモuspto-grants-1987_10