化工社化工社 化学情報印刷レポート · 研究参考用
Chlorine → 2,3-Dichloro-5-(trichloromethyl)pyridine
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Chlorine | HCID 24526 | — |
| 反応物 | 2-Chloro-5-trichloromethylpyridine | HCID 50293 | — |
| 生成物 | 2,3-Dichloro-5-(trichloromethyl)pyridine | HCID 94647 | — |
反応手順
Instead of isolating the 2-chloro-5-(trichloromethyl)-pyridine from this mixture, the above-described mixture is reacted with chlorine according to the conditions of the present invention as described herein to form 2,3-dichloro-5-(trichloromethyl)pyridine. The resulting 2,3-dichloro-5-(trichloromethyl)pyridine is separated from the reaction mixture by distillation, crystal refining, recrystallization from a solvent or a combination thereof.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04701532 |
| 出典データセット | uspto-grants-1987_10 |
| ORD ID | ord-8b9a8af931f642f395be17353d236fdc |
| 出典メモ | uspto-grants-1987_10 |