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HRID 256212作成日:2026年10月27日

Chlorine → 2,3-Dichloro-5-(trichloromethyl)pyridine

https://huagongshe.com/reaction/256212

反応式

関与物質

役割名称HCID仕込み量
反応物ChlorineHCID 24526—
反応物2-Chloro-5-trichloromethylpyridineHCID 50293—
生成物2,3-Dichloro-5-(trichloromethyl)pyridineHCID 94647—

反応手順

Instead of isolating the 2-chloro-5-(trichloromethyl)-pyridine from this mixture, the above-described mixture is reacted with chlorine according to the conditions of the present invention as described herein to form 2,3-dichloro-5-(trichloromethyl)pyridine. The resulting 2,3-dichloro-5-(trichloromethyl)pyridine is separated from the reaction mixture by distillation, crystal refining, recrystallization from a solvent or a combination thereof.

情報源と証拠

DOI10.6084/m9.figshare.5104873.v1
特許番号US04701532
出典データセットuspto-grants-1987_10
ORD IDord-8b9a8af931f642f395be17353d236fdc
出典メモuspto-grants-1987_10