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Trifluoroacetic acid → HCID 178457217、化合物
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Trifluoroacetic acid | HCID 6422 | — |
| 反応物 | N-Methylallylamine | HCID 69391 | — |
| 反応物 | 4-(Trifluoromethyl)benzenesulfonyl chloride | HCID 2777399 | — |
| 反応物 | HCID 178484800 | HCID 178484800 | — |
| 生成物 | HCID 178457217 | HCID 178457217 | — |
反応手順
In analogy to examples 31.5 and 31.6, trans-Methanesulfonic acid 4-(4-methylamino-cyclohexyl)-butyl ester.trifluoro-acetic acid and and 4-trifluoromethyl-phenyl-sulfonylchloride were reacted, followed by treatment with N-allyl-N-methylamine to give trans-N-{4-[4-(Allyl-methyl-amino)-butyl]-cyclohexyl}-N-methyl-4-trifluoromethyl-benzenesulfonamide, MS: 447 (MH+).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US06858651B2 |
| 出典データセット | uspto-grants-2005_02 |
| ORD ID | ord-9b7c69e8bf6440608ef6f7ab93b482bf |
| 出典メモ | uspto-grants-2005_02 |