化工社化工社 化学情報印刷レポート · 研究参考用
Triethylenetetramine → Ethylene carbonate triethylene tetraamine
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Triethylenetetramine | HCID 5565 | — |
| 反応物 | Ethylene carbonate | HCID 7303 | — |
| 反応物 | Potassium Hydroxide | HCID 14797 | — |
| 溶媒 | Toluene | HCID 1140 | — |
| 生成物 | Ethylene carbonate triethylene tetraamine | HCID 86740738 | — |
反応手順
Add 2 g of triethylene tetraamine (with an AV of approximately 1180 mg KOH/g) to 20 ml of toluene in a 250 ml flask fitted with a stirrer, condensor and nitrogen inlet. Add 0.6 g ethylene carbonate to the mixture. Reflux the system for 2.5 hours under N2. Strip the system to yield an ethylene carbonate-triethylene tetraamine adduct having an AV of approximately 670 mg KOH/g.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04702851 |
| 出典データセット | uspto-grants-1987_10 |
| ORD ID | ord-55c355b73fd1451ea2c21d8fa2cecb05 |
| 出典メモ | uspto-grants-1987_10 |