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Diethyl Ether → 5-Norbornene-2-carboxylic acid
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Diethyl Ether | HCID 3283 | — |
| 反応物 | Acrylic Acid | HCID 6581 | — |
| 反応物 | Cyclopentadiene | HCID 7612 | — |
| 生成物 | 5-Norbornene-2-carboxylic acid | HCID 78949 | 82% |
反応手順
49.5 g of acrylic acid was added to 49.9 g of cyclopentadiene and 40 ml of diethyl ether, and a reaction was allowed to react at room temperature for 2 hr with stirring. After the completion of the reaction, the reaction mixture was concentrated and purified by distillation to give 78.0 g (yield: 82%) of an intended product.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05260257 |
| 出典データセット | uspto-grants-1993_11 |
| ORD ID | ord-27035d7ebe8f4b13943e774c599ac188 |
| 出典メモ | uspto-grants-1993_11 |