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N-methyl-4-nitrophenethylamine → 1-(4-nitrophenyl)-4-(N-methyl-N-(2-(4-nitrophenyl)ethyl)amino)piperidine
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | N-methyl-4-nitrophenethylamine | HCID 2794239 | — |
| 反応物 | 1-(4-Nitrophenyl)piperidin-4-one | HCID 3842562 | — |
| 生成物 | 1-(4-nitrophenyl)-4-(N-methyl-N-(2-(4-nitrophenyl)ethyl)amino)piperidine | HCID 19784394 | 52.5% |
反応手順
2.4 g (10.9 mmol) of 1-(4-nitrophenyl)-4-piperidone and 2.0 g (10.9 mmol) of N-methyl-N-(2-(4-nitrophenyl)ethyl)amine were reacted in a similar manner to Example 1. 2.2 g of 1-(4-nitrophenyl)-4-(N-methyl-N-(2-(4-nitrophenyl)ethyl)amino)piperidine were obtained. Melting point 97°-98° C.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05260318 |
| 出典データセット | uspto-grants-1993_11 |
| ORD ID | ord-c87b100564df46948eb0fbf4be09245b |
| 出典メモ | uspto-grants-1993_11 |