関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|
| 反応物 | Benzyl mercaptan | HCID 7509 | — |
| 反応物 | Potassium Carbonate | HCID 11430 | — |
| 反応物 | Benzene, 2-chloro-1,5-dinitro-3-(trifluoromethyl)- | HCID 67851 | — |
| 溶媒 | Dimethylformamide | HCID 6228 | — |
| 生成物 | 2-Benzylthio-3,5-dinitrobenzotrifluoride | HCID 13581600 | — |
反応手順
67.6 g of 2-chloro-3,5-dinitrobenzotrifluoride are dissolved in 150 ml of N,N-dimethylformamide (DMF) and the mixture is treated with 35.9 g of solid potassium carbonate, treated dropwise with 31 g of benzylmercaptan in 200 ml of DMF with stirring at 0° C., and subsequently stirred for a further 16 hours at room temperature, while cooling.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 特許番号 | US05260423 |
|---|
| 出典データセット | uspto-grants-1993_11 |
|---|
| ORD ID | ord-d6b8c35d48a6424c99ef491dfd6d32b1 |
|---|
| 出典メモ | uspto-grants-1993_11 |
|---|
