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Phenyl isocyanate → Acetanilide
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Phenyl isocyanate | HCID 7672 | — |
| 反応物 | Isocyanate | HCID 105034 | — |
| 溶媒 | Acetic Acid | HCID 176 | — |
| 生成物 | Acetanilide | HCID 904 | — |
| 生成物 | Carbanilide | HCID 7595 | — |
反応手順
1.19 g phenyl isocyanate and 0.6 g acetic acid were reacted in a 1:1 isocyanate:acetic acid molar ratio. The reaction, product isolation and analysis were conducted as in Example 1. 0.45 g diphenyl urea and 0.9 g acetanilide were obtained.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05260483 |
| 出典データセット | uspto-grants-1993_11 |
| ORD ID | ord-c3d0a39d32c549c79511e491efbc746a |
| 出典メモ | uspto-grants-1993_11 |