4-Ethylpyridine → HCID 19783323、化合物

反応式

[CH2:1]([C:3]1[CH:8]=[CH:7][N:6]=[CH:5][CH:4]=1)[CH3:2].[F:9][C:10]([F:21])([F:20])[C:11]1[CH:12]=[C:13]([CH:17]=[CH:18][CH:19]=1)[CH2:14][CH2:15]Br>>[F:9][C:10]([F:21])([F:20])[C:11]1[CH:12]=[C:13]([CH2:14][CH2:15][CH:1]([C:3]2[CH:8]=[CH:7][N:6]=[CH:5][CH:4]=2)[CH3:2])[CH:17]=[CH:18][CH:19]=1

参加物

反応物 2

HCID 108224-Ethylpyridine

HCID 5945351-(2-Bromoethyl)-3-(trifluoromethyl)benzene

生成物 1

HCID 19783323HCID 19783323、化合物収率 15.3%

実験手順

1.0 g (9.35 mmol) of 4-ethylpyridine and 2.37 g (9.35 mmol) of 3-trifluoromethylphenethyl bromide were reacted in the same manner as in Example 1. The reaction product was purified to obtain 0.40 g of the desired compound (yield: 15.3%).

後処理

customThe reaction product was purified

出典と根拠

ORDレコード: ord-b4d1128d52804dd5ae28aba2497326e8
出典データセット: uspto-grants-1993_11
DOI: 10.6084/m9.figshare.5104873.v1
特許番号: US05262420

反応ノート

読み込み中…