化工社化工社 化学情報印刷レポート · 研究参考用
4-Ethylpyridine → 1-(4-Fluorophenyl)-3-(4-pyridyl)-butane
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 4-Ethylpyridine | HCID 10822 | — |
| 反応物 | 4-Fluorophenethyl bromide | HCID 573153 | — |
| 生成物 | 1-(4-Fluorophenyl)-3-(4-pyridyl)-butane | HCID 19783359 | 77.9% |
反応手順
1.0 g (9.35 mmol) of 4-ethylpyridine and 1.90 g (9.35 mmol) of 4-fluorophenethyl bromide were reacted in the same manner as in Example 1. The reaction product was purified to obtain 1.67 g of the desired compound (yield: 77.9%). The resulting compound was identified as 1-(4-fluorophenyl)-3-(4-pyridyl)-butane (hereinafter referred to as compound 5) by the following analytical results.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05262420 |
| 出典データセット | uspto-grants-1993_11 |
| ORD ID | ord-e663950e935943889a2b643fbec43c52 |
| 出典メモ | uspto-grants-1993_11 |