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4-Ethylpyridine → 1-(4-Methylphenyl)-3-(4-pyridyl)-butane
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 4-Ethylpyridine | HCID 10822 | — |
| 反応物 | 4-Methylphenethyl bromide | HCID 570680 | — |
| 生成物 | 1-(4-Methylphenyl)-3-(4-pyridyl)-butane | HCID 19783304 | 98.4% |
反応手順
1.0 g (9.35 mmol) of 4-ethylpyridine and 1.86 g (9.35 mmol) of 4-methylphenethyl bromide were reacted in the same manner as in Example 1. The reaction product was purified to obtain 2.07 g of the desired compound (yield: 98.4%). The resulting compound was identified as 1-(4-methylphenyl)-3-(4-pyridyl)-butane (hereinafter referred to as compound 7) by the following analytical results.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05262420 |
| 出典データセット | uspto-grants-1993_11 |
| ORD ID | ord-b94f3e175a914bafa6eb4e78d47d9684 |
| 出典メモ | uspto-grants-1993_11 |