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4-Ethylpyridine → 1-(2,6-Dichlorophenyl)-3-(4-pyridyl)butane
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 4-Ethylpyridine | HCID 10822 | — |
| 反応物 | 2-(2-Bromoethyl)-1,3-dichlorobenzene | HCID 13480195 | — |
| 生成物 | 1-(2,6-Dichlorophenyl)-3-(4-pyridyl)butane | HCID 19783313 | 55.3% |
反応手順
1.0 g (9.35 mmol) of 4-ethylpyridine and 2.37 g (9.35 mmol) of 2,6-dichlorophenethyl bromide were reacted in the same manner as in Example 1. The reaction product was purified to obtain 1.45 g of the desired compound (yield: 55.3%). The resulting compound was identified as 1-(2,6-dichlorophenyl)-3-(4-pyridyl)-butane (hereinafter referred to as compound 11) by the following analytical results.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05262420 |
| 出典データセット | uspto-grants-1993_11 |
| ORD ID | ord-ee4c7f6b2d9949818626607b3a34d2d8 |
| 出典メモ | uspto-grants-1993_11 |