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Iodoethane → 1-Phenyl-3-(3-n-propyl-4-pyridyl)butane
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Iodoethane | HCID 6340 | — |
| 反応物 | 1-Phenyl-3-(3-methyl-4-pyridyl)butane | HCID 19783297 | — |
| 反応物 | Lithium diisopropylamine | HCID 45051747 | — |
| 生成物 | 1-Phenyl-3-(3-n-propyl-4-pyridyl)butane | HCID 19783320 | 15.6% |
反応手順
2.1 g (9.35 mmol) of 1-phenyl-3-(3-methyl-4-pyridyl)butane, 1.46 g (9.35 mmol) of ethyl iodide and 2 equivalent of lithium-diisopropylamine were reacted in the same manner as in Example 1. The reaction product was purified to obtain 0.37 g of the desired compound (yield: 15.6%).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05262420 |
| 出典データセット | uspto-grants-1993_11 |
| ORD ID | ord-050c0500979a4433a4718a4be18e859c |
| 出典メモ | uspto-grants-1993_11 |