(3-Bromopropyl)benzene → 1-Phenyl-4-(3-ethyl-4-pyridyl)-butane

HRID 257480

反応式

HRID 257480 の反応式
[CH2:1]([C:3]1[CH:4]=[N:5][CH:6]=[CH:7][C:8]=1[CH3:9])[CH3:2].Br[CH2:11][CH2:12][CH2:13][C:14]1[CH:19]=[CH:18][CH:17]=[CH:16][CH:15]=1>>[C:14]1([CH2:13][CH2:12][CH2:11][CH2:9][C:8]2[CH:7]=[CH:6][N:5]=[CH:4][C:3]=2[CH2:1][CH3:2])[CH:19]=[CH:18][CH:17]=[CH:16][CH:15]=1

参加物

3

反応物 2

HCID 12503(3-Bromopropyl)benzeneHCID 682543-Ethyl-4-methylpyridine

生成物 1

HCID 148837881-Phenyl-4-(3-ethyl-4-pyridyl)-butane収率 87.8%

実験手順

1.83 g (15.1 mmol) of 3-ethyl-4-methylpyridine and 3.0 g (15.1 mmol) of 1-bromo-3-phenylpropane were reacted in the same manner as in Example 26. The reaction product was purified to obtain 3.17 g of the desired compound (yield: 87.8%).

後処理

  1. customThe reaction product was purified

出典と根拠

ORDレコード
ord-9ceaedd5a72a41bd9770532296aea3d1
出典データセット
uspto-grants-1993_11
特許番号
US05262420

関連ノート

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