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3-Ethyl-4-methylpyridine → 1-(3-Trifluoromethylphenyl)-4-(3-ethyl-4-pyridyl)-butane
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 3-Ethyl-4-methylpyridine | HCID 68254 | — |
| 反応物 | 1-(3-Bromopropyl)-3-(trifluoromethyl)benzene | HCID 19783367 | — |
| 生成物 | 1-(3-Trifluoromethylphenyl)-4-(3-ethyl-4-pyridyl)-butane | HCID 14883795 | 80.5% |
反応手順
1.83 g (15.1 mmol) of 3-ethyl-4-methylpyridine and 4.03 g (15.1 mmol) of 1-bromo-3-(3-trifluoromethylphenyl) propane were reacted in the same manner as in Example 26. The reaction compound was purified to obtain 3.73 g of the desired compound (yield: 80.5%).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05262420 |
| 出典データセット | uspto-grants-1993_11 |
| ORD ID | ord-3b9d8da1be95426a9dea1dec64ae6189 |
| 出典メモ | uspto-grants-1993_11 |