化工社化工社 化学情報印刷レポート · 研究参考用
Pyridine, 4-ethyl-3-methyl- → 1-(3,4-Dichlorophenyl)-4-(3-methyl-4-pyridyl)-pentane
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Pyridine, 4-ethyl-3-methyl- | HCID 34088 | — |
| 反応物 | 4-(3-bromopropyl)-1,2-dichloroBenzene | HCID 21962957 | — |
| 生成物 | 1-(3,4-Dichlorophenyl)-4-(3-methyl-4-pyridyl)-pentane | HCID 14883798 | 37.3% |
反応手順
1.83 g (15.1 mmol) of 3-methyl-4-ethylpyridine and 4.05 g (15.1 mmol) of 1-bromo-3-(3,4-dichlorophenyl)-propane were reacted in the same manner as in Example 26. The reaction product was purified to obtain 1.73 g of the desired compound (yield:37.3%).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05262420 |
| 出典データセット | uspto-grants-1993_11 |
| ORD ID | ord-b01cad38ee28421c9c16eb0c9843d045 |
| 出典メモ | uspto-grants-1993_11 |