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HRID 257491作成日:2026年10月26日

Benzyl acetone → (E)-1-(3-ethyl-4-pyridyl)-2-methyl-4-phenyl-1-butene

https://huagongshe.com/reaction/257491

反応式

関与物質

役割名称HCID仕込み量
反応物Benzyl acetoneHCID 17355—
反応物3-Ethyl-4-methylpyridineHCID 68254—
生成物(E)-1-(3-ethyl-4-pyridyl)-2-methyl-4-phenyl-1-buteneHCID 1488380369.5%

反応手順

The procedure of Example 41 was repeated with the exception that 3.5 g of benzyl acetone in place of cinnamic aldehyde and 2.26 g of 3-ethyl-4-methylpyridine were used in Example 41, to obtain 3.26 g (yield: 59.8%) of (E)-1-(3-ethyl-4-pyridyl)-2-methyl-4-phenyl -1-butene (hereinafter referred to as compound 55) and o.95 g (yield: 17.4%) of (Z)-1-(3-ethyl-4-pyridyl)-2-methyl-4-phenyl-1-butene (hereinafter referred to as compound 56). The analytical results are shown below.

情報源と証拠

DOI10.6084/m9.figshare.5104873.v1
特許番号US05262420
出典データセットuspto-grants-1993_11
ORD IDord-8b990d7f82d54f9b834fc6ef6159ea3e
出典メモuspto-grants-1993_11