反応式
C1(S[CH2:7][C:8]2[C:17]3[C:12](=[CH:13][CH:14]=[C:15]([C:18]4[CH:23]=[CH:22][CH:21]=[CH:20][C:19]=4[O:24][CH3:25])[CH:16]=3)[NH:11][C:10]([CH3:27])([CH3:26])[CH:9]=2)CCCC1.BrCC1[C:39]2[C:34](=[CH:35][CH:36]=[C:37](C3C=CC=CC=3OC)[CH:38]=2)[NH:33]C(C)(C)C=1.C(=O)([O-])[O-].[K+].[K+].C1(S)CCCC1>>[CH3:25][O:24][C:19]1[CH:20]=[CH:21][CH:22]=[CH:23][C:18]=1[C:15]1[CH:16]=[C:17]2[C:12](=[CH:13][CH:14]=1)[NH:11][C:10]([CH3:26])([CH3:27])[CH:9]=[C:8]2[CH2:7][NH:33][C:34]1[CH:39]=[CH:38][CH:37]=[CH:36][CH:35]=1参加物
5
反応物 4
生成物 1
実験手順
4-Cyclopentylsulfanylmethyl-6-(2-methoxyphenyl)-2,2-dimethyl-1,2-dihydroquinoline 80 mg of 4-bromomethyl-6-(2-methoxyphenyl)-2,2-dimethyl-1,2-dihydroquinoline, 69 mg of potassium carbonate, and 48 μL of cyclopentyl mercaptan reacted to give 7 mg of the title compound as a foam.
出典と根拠
- ORDレコード
- ord-099e4ecc4f544ddfb38a5c2022523af5
- 出典データセット
- uspto-grants-2005_02
- 特許番号
- US06858627B2
関連ノート
読み込み中…