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HRID 258347作成日:2026年10月25日

Cyanuric chloride → Anthraquinone

https://huagongshe.com/reaction/258347

反応式

関与物質

役割名称HCID仕込み量
反応物Cyanuric chlorideHCID 7954—
反応物3-Aminobenzenesulfonic acidHCID 8474—
反応物1-Amino-2-(3'-amino-4'-sulfophenoxy)-4-(4-sulfophenylthio)anthraquinoneHCID 14717378—
生成物AnthraquinoneHCID 6780—

反応手順

1-Amino-2-(3'-amino-4'-sulfophenoxy)-4-(4'-sulfophenylthio)anthraquinone (6 parts), cyanuric chloride (1.8 parts) and 1-aminobenzene-4-β-sulfatoethylsulfone (2.8 parts) were subjected to condensation reactions one after another in an aqueous medium in a conventional manner, followed by a successive condensation reaction with 3-aminobenzenesulfonic acid (1.7 parts) at 50° to 70° C. under a weak acid condition. Thereafter, salting out of the reaction mixture gave an anthraquinone compound of following formula (free acid form). ##STR117##

情報源と証拠

DOI10.6084/m9.figshare.5104873.v1
特許番号US05266696
出典データセットuspto-grants-1993_11
ORD IDord-ec448160f7474ac0a180e86215289add
出典メモuspto-grants-1993_11