化工社化工社 化学情報印刷レポート · 研究参考用
Formaldehyde → Formaldehyde urea silicate
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Formaldehyde | HCID 712 | — |
| 反応物 | Sulfuric Acid | HCID 1118 | — |
| 反応物 | Urea | HCID 1176 | — |
| 反応物 | Urea silicate | HCID 86734903 | — |
| 生成物 | Formaldehyde urea silicate | HCID 86734902 | — |
反応手順
The said urea silicate is added to an aqueous solution of formaldehyde in the ratio of 1:1.5 mols, mixed, and the urea silicate goes into solution. The unreacted silicic acid is removed by filtration. About 15% to 25% of the said silicic acid did not chemically react with said urea. To the clear aqueous solution of urea silicate and formaldehyde is added a dilute solution of sulfuric acid until the pH is 4 to 5, then said solution is heated to 70° to 110° C. for 20 to 80 minutes, until the desired viscosity is obtained, thereby producing poly (formaldehyde urea silicate) resin, which is clear in color and may be produced as a thick liquid or as a solid. The said solid resin may be heated to 70° to 80° C. and molded into useful objects.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04033935 |
| 出典データセット | uspto-grants-1977_07 |
| ORD ID | ord-5b3dde485409449bbb73e13a53eee45f |
| 出典メモ | uspto-grants-1977_07 |