化工社化工社 化学情報印刷レポート · 研究参考用
N-(4-Chloro-2-methylphenyl)formamide → Formamide, N-(2-methylphenyl)-
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | N-(4-Chloro-2-methylphenyl)formamide | HCID 30815 | — |
| 溶媒 | Methanol | HCID 887 | — |
| 生成物 | Formamide, N-(2-methylphenyl)- | HCID 7202 | — |
反応手順
Splitting of the 2-formylamino-5-chlorotoluene, formed on chlorination of 2-formylaminotoluene, with methanol is performed at a temperature of between 20° and 60° C., preferably at between 25° and 30° C. The reaction duration is about 1 to 2 hours.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04034043 |
| 出典データセット | uspto-grants-1977_07 |
| ORD ID | ord-0e5282493e114da597907408c0830fb6 |
| 出典メモ | uspto-grants-1977_07 |