化工社化工社 化学情報印刷レポート · 研究参考用
Hydrochloric Acid → Di-n-decyl-n-tetradecylmethylchloride
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Hydrochloric Acid | HCID 313 | — |
| 反応物 | Calcium Chloride | HCID 5284359 | — |
| 反応物 | Di-n-decyl-n-tetradecylcarbinol | HCID 19690406 | — |
| 溶媒 | Dichloromethane | HCID 6344 | — |
| 生成物 | Di-n-decyl-n-tetradecylmethylchloride | HCID 19690403 | — |
反応手順
One mole of di-n-decyl-n-tetradecylcarbinol is added to 0.2 liters of methylene chloride and 0.32 moles calcium chloride. Approximately 1.5 moles of HCl gas is slowly bubbled through the solution. The product mixture is then washed with 1 liter of a 10% sodium carbonate solution. The organic layer is dried with magnesium sulfate and the methylene chloride is evaporated off to give di-n-decyl-n-tetradecyl-methylchloride.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05728907 |
| 出典データセット | uspto-grants-1998_03 |
| ORD ID | ord-3272ce8059be4591a93fe2fa3200dcab |
| 出典メモ | uspto-grants-1998_03 |