関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|
| 反応物 | Water | HCID 962 | — |
| 反応物 | p-Toluenesulfonic acid | HCID 6101 | — |
| 反応物 | Isodecanol | HCID 32898 | — |
| 溶媒 | O-Xylene | HCID 7237 | — |
| 生成物 | Isodecyl acrylate | HCID 14899 | — |
反応手順
To 157 g isodecyl alcohol in 200 ml xylene is added 117 g AA, 1.0 g HQ and 2.0Q PTSA. The reaction mixture is heated for 2 hrs. at reflux (140° C) while the water of reaction is collected (17 ml). The reaction mixture is cooled and the xylene removed under reduced pressure to give 250 g isodecyl acrylate. The analytical data for this acrylate is shown below.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 特許番号 | US04035409 |
|---|
| 出典データセット | uspto-grants-1977_07 |
|---|
| ORD ID | ord-7aeb45784b7e46019546e24d9d59e0ae |
|---|
| 出典メモ | uspto-grants-1977_07 |
|---|
