Morpholine → N-(4,5,6,7-tetrahydrobenzo[b]thien-4-yl)-4-morpholinecarboxamide
反応式
[S:1]1[CH:5]=[CH:4][C:3]2[CH:6]([N:10]=[C:11]=[O:12])[CH2:7][CH2:8][CH2:9][C:2]1=2.[NH:13]1[CH2:18][CH2:17][O:16][CH2:15][CH2:14]1>C(OCC)C>[S:1]1[CH:5]=[CH:4][C:3]2[CH:6]([NH:10][C:11]([N:13]3[CH2:18][CH2:17][O:16][CH2:15][CH2:14]3)=[O:12])[CH2:7][CH2:8][CH2:9][C:2]1=2参加物
4
実験手順
In the manner outlined in Example 6, except for using diethyl ether instead of methylene chloride, 4,5,6,7-tetrahydrobenzo[b]thien-4-yl isocyanate is allowed to react with morpholine to give N-(4,5,6,7-tetrahydrobenzo[b]thien-4-yl)-4-morpholinecarboxamide, which melts at 152° C. to 154° C.
出典と根拠
- ORDレコード
- ord-b96acfb582c947279189dea53382f095
- 出典データセット
- uspto-grants-1977_07
- 特許番号
- US04036979
反応ノート
読み込み中…