化工社化工社 化学情報印刷レポート · 研究参考用
Potassium Hydroxide → L-(-)-Ornithine
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Potassium Hydroxide | HCID 14797 | — |
| 反応物 | Ornithine hydrochloride | HCID 76654 | — |
| 溶媒 | Ethanol | HCID 702 | — |
| 生成物 | L-(-)-Ornithine | HCID 6262 | 98.7% |
反応手順
Into the reaction apparatus used in Example 1, 160 g of ethyl alcohol, 16.8 g of ornithine hydrochloride and 5.6 g of potassium hydroxide were added. The resulting mixture was reacted for 3 hours, refluxing the solvent, while being stirred. After the reaction was over, the resultant product was cooled to room temperature and then the by-product potassium chloride was filtered off. Then the solvent was distilled off from the resultant product under reduced pressure to obtain 13.0 g of ornithine in a syrupy state.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04038287 |
| 出典データセット | uspto-grants-1977_07 |
| ORD ID | ord-618c09d176a94c05b137be44b681cd93 |
| 出典メモ | uspto-grants-1977_07 |