Phosgene → 27676-61-5

HRID 259479ノート

反応式

HRID 259479 の反応式
[CH:1]([N:4]=[C:5]([CH3:7])[CH3:6])([CH3:3])[CH3:2].C(N(CC)CC)C.[C:15](Cl)([Cl:17])=[O:16]>C(Cl)Cl>[C:5]([N:4]([CH:1]([CH3:3])[CH3:2])[C:15]([Cl:17])=[O:16])([CH3:7])=[CH2:6]

参加物

5

反応物 3

HCID 6371PhosgeneHCID 8471TriethylamineHCID 1378922-Propanamine, N-(1-methylethylidene)-

生成物 1

HCID 2142189827676-61-5

試薬・触媒・溶媒 1

HCID 6344Dichloromethane溶媒

実験手順

99 parts of acetone isopropylimine and 94 parts of triethylamine are dissolved in 400 parts of methylene chloride, and the whole reacted with 120 parts of phosgene at a temperature of 30° to 40° C., as described in Example 1. After isolation, 131 parts (81% of the theory) of N-isopropenyl-N-isopropylcarbamyl chloride is obtained having a boiling point of 69° C. at 3 mm.

出典と根拠

ORDレコード
ord-ce74260db5984f96846981140cc39aa4
出典データセット
uspto-grants-1977_07
特許番号
US04038311

反応ノート

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