化工社化工社 化学情報印刷レポート · 研究参考用
Ammonium Acetate → Ethyl 3-amino-2-chloro-4-methyl-2-pentenoate
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Ammonium Acetate | HCID 517165 | — |
| 反応物 | Ethyl 2-chloro-4-methyl-3-oxopentanoate | HCID 9877606 | — |
| 溶媒 | Methanol | HCID 887 | — |
| 生成物 | Ethyl 3-amino-2-chloro-4-methyl-2-pentenoate | HCID 86749531 | 88% |
反応手順
59.5 g (0.31 mol) of ethyl 2-chloro-4-methyl-3-oxo-pentanoate are reacted with 59.8 g (0.78 mol) of ammonium acetate in 120 ml of methanol and worked up in analogy to Example 2. Yield: 88.0% [GC]
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05523404 |
| 出典データセット | uspto-grants-1996_06 |
| ORD ID | ord-890cfefd4e874537ba30aac96aa2c748 |
| 出典メモ | uspto-grants-1996_06 |