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Pyridine → Cotinine
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Pyridine | HCID 1049 | — |
| 反応物 | Succinic anhydride | HCID 7922 | — |
| 反応物 | 3'-Hydroxycotinine, trans- | HCID 107963 | — |
| 溶媒 | Dimethylformamide | HCID 6228 | — |
| 生成物 | Cotinine | HCID 854019 | — |
反応手順
Cotinine hemisuccinate was prepared by dissolving 19 mg of trans-3'-hydroxycotinine in 1 ml of dimethylformamide (Aldrich). 21 mg of succinic anhydride (Aldrich) were added, followed by 15 μl of pyridine (Aldrich). The mixture was incubated overnight at 45° C.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05527686 |
| 出典データセット | uspto-grants-1996_06 |
| ORD ID | ord-7c2cd0ad0eb24c1c8ca3ae468fdcc9cc |
| 出典メモ | uspto-grants-1996_06 |