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Phosphorus oxychloride → 2-(2,6-Diethyl-3-methylanilino)-2-imidazoline
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Phosphorus oxychloride | HCID 24813 | — |
| 反応物 | N-Acetylimidazolidinone | HCID 79350 | — |
| 反応物 | m-Toluidine, 2,6-diethyl- | HCID 144235 | — |
| 生成物 | 2-(2,6-Diethyl-3-methylanilino)-2-imidazoline | HCID 22401593 | — |
反応手順
2,6-Diethyl-3-methyl aniline is reacted with N-acetyl-2-imidazolidinone in the presence of POCl3 to produce the imidazoline. This intermediate is treated with sodium hydroxide and water to remove the acetyl group and yield the name compound (VI).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05527830 |
| 出典データセット | uspto-grants-1996_06 |
| ORD ID | ord-269305ddd5f9418ea022ac43d34bd89e |
| 出典メモ | uspto-grants-1996_06 |