化工社化工社 化学情報印刷レポート · 研究参考用
Chlorotrimethylsilane → 2-Benzyl-2-trimethylsilyl-1,3-dithiane
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Chlorotrimethylsilane | HCID 6397 | — |
| 反応物 | 2-Benzyl-1,3-dithiane | HCID 300291 | — |
| 生成物 | 2-Benzyl-2-trimethylsilyl-1,3-dithiane | HCID 10469008 | 75% |
反応手順
The title compound of this step was prepared in 75% yield, by the procedure described in JACS 89, (1967), 4347 by E. J. Corey, et al., using 2-benzyl-1,3-dithiane and trimethylsilyl chloride. The product was recrystallized from diethyl ether/pentane.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05529988 |
| 出典データセット | uspto-grants-1996_06 |
| ORD ID | ord-157274fec4e5454391c7c93903080036 |
| 出典メモ | uspto-grants-1996_06 |