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Homophthalic acid → 3,3-dimethyl-5-oxo-2,3-dihydro-5H-thiazolo[3,2-b]isoquinoline
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Homophthalic acid | HCID 66643 | — |
| 反応物 | Sodium Acetate | HCID 517045 | — |
| 反応物 | 2-Amino-2-methylpropane-1-thiol | HCID 521040 | — |
| 溶媒 | 1,2-Dichlorobenzene | HCID 7239 | — |
| 生成物 | 3,3-dimethyl-5-oxo-2,3-dihydro-5H-thiazolo[3,2-b]isoquinoline | HCID 12593065 | — |
反応手順
By following the same procedure as in Example 49 using a mixture of 240 mg. of 2-carboxymethylbenzoic acid, 300 mg. of 2-amino-2-methylpropanethiol, 164 mg. of sodium acetate, and 5 ml. of o-dichlorobenzene, 120 mg. of 3,3-dimethyl-5-oxo-2,3-dihydro-5H-thiazolo[3,2-b]isoquinoline was obtained.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04163844 |
| 出典データセット | uspto-grants-1979_08 |
| ORD ID | ord-64cfce68ca0c405c91b0742af24d77f8 |
| 出典メモ | uspto-grants-1979_08 |