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Nitric Acid → Dibismuth molybdenum hexaoxide
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Nitric Acid | HCID 944 | — |
| 反応物 | Ammonium Hydroxide | HCID 14923 | — |
| 反応物 | Azane;molybdenum;tetracosahydrate | HCID 25488 | — |
| 反応物 | Bismuth nitrate | HCID 107711 | — |
| 溶媒 | Water | HCID 962 | — |
| 生成物 | Dibismuth molybdenum hexaoxide | HCID 159680 | — |
反応手順
14.55 g Bi(NO3)3.5H2O was dissolved in 100 ml. of a 10 percent HNO3 aqueous solution. 7.95 g of (NH4)Mo7O24.4H2O was dissolved in 100 ml. H2O with heating. The bismuth nitrate solution was then slowly added to the ammonium heptamolybdate solution with constant stirring. The pH was then adjusted to 2.5 to 3 by the addition of NH4OH. The mixture was stirred for about one hour, thereby yielding a bismuth molybdate slurry.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04148757 |
| 出典データセット | uspto-grants-1979_04 |
| ORD ID | ord-81df126905674916a2ca429adb571ac4 |
| 出典メモ | uspto-grants-1979_04 |