化工社化工社 化学情報印刷レポート · 研究参考用
2-Mercaptoethanol → 2-(6-Carboxyhexyl)-4-(2-hydroxyethylthio)cyclopent-2-en-1-one
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 2-Mercaptoethanol | HCID 1567 | — |
| 反応物 | ACMC-20apjz | HCID 3690897 | — |
| 反応物 | Sodium Methoxide | HCID 10942334 | — |
| 溶媒 | Methanol | HCID 887 | — |
| 生成物 | 2-(6-Carboxyhexyl)-4-(2-hydroxyethylthio)cyclopent-2-en-1-one | HCID 23346654 | — |
反応手順
In the manner of Example 281 a methanol solution of 2-(6-carboxyhexyl)-4-hydroxycyclopent-2-en-1-one [Prostaglandins, 3, 921 (1973)] and β-mercaptoethanol is treated with sodium methoxide solution, acidified, concentrated, and extracted to provide the subject compound as an oil.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04165331 |
| 出典データセット | uspto-grants-1979_08 |
| ORD ID | ord-30160fcc15e5467ca5ce4ce942634e16 |
| 出典メモ | uspto-grants-1979_08 |