Hydrochloric Acid → 3-Amino-7-benzamidoheptan-2-one hydrochloride

HRID 261618ノート

反応式

HRID 261618 の反応式
C([NH:9][CH:10]([CH2:14][CH2:15][CH2:16][CH2:17][NH:18][C:19](=[O:26])[C:20]1[CH:25]=[CH:24][CH:23]=[CH:22][CH:21]=1)[C:11](=[O:13])[CH3:12])(=O)C1C=CC=CC=1.[ClH:27]>>[ClH:27].[NH2:9][CH:10]([CH2:14][CH2:15][CH2:16][CH2:17][NH:18][C:19](=[O:26])[C:20]1[CH:21]=[CH:22][CH:23]=[CH:24][CH:25]=1)[C:11](=[O:13])[CH3:12]

参加物

3

反応物 2

HCID 313Hydrochloric AcidHCID 127698383,7-Dibenzamidoheptan-2-one

生成物 1

HCID 203945683-Amino-7-benzamidoheptan-2-one hydrochloride収率 34.2%

実験手順

3,7-Dibenzamidoheptan-2-one (91.11 g, 0.258 mol) was hydrolysed in a sealed tube with concentrated HCl for 3 hours at 160° (oil bath). The solution was extracted with ether and evaporated to dryness to give 3-amino-7-benzamidoheptan-2-one hydrochloride (25.01 g, 34.2%).

後処理

  1. extractionThe solution was extracted with ether
  2. customevaporated to dryness

出典と根拠

ORDレコード
ord-0dfa7767110e41af95b6413b4d86f4d6
出典データセット
uspto-grants-1979_08
特許番号
US04166184

反応ノート

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