化工社化工社 化学情報印刷レポート · 研究参考用
alpha-(p-Bromophenyl)-alpha-phenyl-1-(toluene-p-sulphonyl)imidazole-2-methanol → bis(4-bromophenyl)(1H-imidazol-2-yl)methanol
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | alpha-(p-Bromophenyl)-alpha-phenyl-1-(toluene-p-sulphonyl)imidazole-2-methanol | HCID 11838798 | — |
| 反応物 | alpha,alpha-Bis(p-bromophenyl)-1-(toluene-p-sulphonyl)imidazole-2-methanol | HCID 12433921 | — |
| 生成物 | bis(4-bromophenyl)(1H-imidazol-2-yl)methanol | HCID 12433872 | — |
反応手順
Using the procedure described in Example IB but substituting an equivalent amount of α,α-bis(p-bromophenyl)-1-(toluene-p-sulphonyl)imidazole-2-methanol for the α-(p-bromophenyl)-α-phenyl-1-(toluene-p-sulphonyl)imidazole-2-methanol, α,α-bis(p-bromophenyl)imidazole-2-methanol was obtained. Its melting point was 192°-194° C. after crystallisation from isopropyl alcohol.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04152441 |
| 出典データセット | uspto-grants-1979_05 |
| ORD ID | ord-2d86235c0e684be8a9c7bf6c439e6a00 |
| 出典メモ | uspto-grants-1979_05 |