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alpha-(p-Bromophenyl)-alpha-phenyl-1-(toluene-p-sulphonyl)imidazole-2-methanol → (2-chlorophenyl)(1H-imidazol-2-yl)phenylmethanol
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | alpha-(p-Bromophenyl)-alpha-phenyl-1-(toluene-p-sulphonyl)imidazole-2-methanol | HCID 11838798 | — |
| 反応物 | (2-chlorophenyl){1-[(4-methylphenyl)sulfonyl]-1H-imidazol-2-yl}phenylmethanol | HCID 12433918 | — |
| 生成物 | (2-chlorophenyl)(1H-imidazol-2-yl)phenylmethanol | HCID 12433860 | — |
反応手順
Using the procedure described in Example IB but substituting an equivalent amount of α-(o-chlorophenyl)-α-phenyl-1-(toluene-p-sulphonyl)imidazole-2-methanol for the α-(p-bromophenyl)-α-phenyl-1-(toluene-p-sulphonyl)imidazole-2-methanol, α-(o-chlorophenyl)-α-phenylimidazole-2-methanol was obtained. Its melting point was 186°-188° C. after crystallisation from isopropyl alcohol.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04152441 |
| 出典データセット | uspto-grants-1979_05 |
| ORD ID | ord-bfa6a586ef56492db00b25efd266f1ef |
| 出典メモ | uspto-grants-1979_05 |