2-Hydroxy-2-phenylcyclopentylamine hydrochloride → HCID 178479598、化合物
反応式
[ClH:1].[C:2]1([C@H:8]2CCC[C@H:9]2[NH2:13])[CH:7]=[CH:6][CH:5]=CC=1.Cl.[OH:15][C:16]1([C:22]2[CH:27]=[CH:26][CH:25]=[CH:24][CH:23]=2)[CH2:20][CH2:19][CH2:18][CH:17]1[NH2:21]>>[ClH:1].[NH:13]1[CH2:9][CH2:8][CH2:2][CH2:7][CH2:6][C:5]1=[N:21][CH:17]1[CH2:18][CH2:19][CH2:20][C:16]1([C:22]1[CH:27]=[CH:26][CH:25]=[CH:24][CH:23]=1)[OH:15]参加物
3
実験手順
Following the procedure described in Example 1, only substituting for cis-2-phenylcyclopentylamine hydrochloride an appropriate amount of 2-hydroxy-2-phenylcyclopentylamine hydrochloride and employing a reaction time of 47 days the desired product was obtained, M.P.261°-262° C.
後処理
- customa reaction time of 47 days
出典と根拠
- ORDレコード
- ord-33369350f4e54196bab5aa16e7740b4e
- 出典データセット
- uspto-grants-1979_05
- 特許番号
- US04153235
反応ノート
読み込み中…