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2-Nitrophenol → 1-(Cyclopentyloxy)-2-nitrobenzene
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 2-Nitrophenol | HCID 6947 | — |
| 反応物 | Bromocyclopentane | HCID 8728 | — |
| 生成物 | 1-(Cyclopentyloxy)-2-nitrobenzene | HCID 22164473 | — |
反応手順
In a similar manner as in Example 1, bromocyclopentane was reacted with o-nitrophenol to yield 2-cyclopentoxynitrobenzene; which was reduced to the corresponding aniline; then reacted with N-methylol-5-methylpyrrolidone to form the corresponding N-5-methyl-N-methylenepyrrolidonyl derivative; which was acylated with chloroacetyl chloride to form the desired product.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04153446 |
| 出典データセット | uspto-grants-1979_05 |
| ORD ID | ord-59c6a960f43e4430b964afb2e83311fb |
| 出典メモ | uspto-grants-1979_05 |