化工社化工社 化学情報印刷レポート · 研究参考用
1-Cyano-2-ethoxy-2-methylaminoethylene → HCID 178483853、化合物
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 1-Cyano-2-ethoxy-2-methylaminoethylene | HCID 73683202 | — |
| 反応物 | HCID 178433288 | HCID 178433288 | — |
| 溶媒 | Pyridine | HCID 1049 | — |
| 生成物 | HCID 178483853 | HCID 178483853 | — |
反応手順
4-Methyl-5-[(2-aminoethyl)thiomethyl]imidazole (3.5 g) was added to a solution of 1-cyano-2-ethoxy-2-methylaminoethylene in pyridine (3.1 g) and the solution was stirred for 5 hours at 100°. The product was chromatographed on a column of neutral alumina with elution by chloroform/ethyl acetate (1:1) to give the title compound as a glass.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04153704 |
| 出典データセット | uspto-grants-1979_05 |
| ORD ID | ord-f361e15054704f7da7f4c14e7d6be3a3 |
| 出典メモ | uspto-grants-1979_05 |