反応式
[CH:1]([N:4]([CH:16]([CH3:18])[CH3:17])[CH2:5][CH2:6][CH:7]([C:10]1[CH:15]=[CH:14][CH:13]=[CH:12][N:11]=1)[C:8]#[N:9])([CH3:3])[CH3:2].[CH:19]([N:22]([CH:34]([CH3:36])[CH3:35])[CH2:23][CH2:24]C(C1C=CC=CC=1)C#N)([CH3:21])[CH3:20]>>[CH:16]([N:4]([CH:1]([CH3:3])[CH3:2])[CH2:5][CH2:6][C:7]([CH2:24][CH2:23][N:22]([CH:34]([CH3:36])[CH3:35])[CH:19]([CH3:21])[CH3:20])([C:10]1[CH:15]=[CH:14][CH:13]=[CH:12][N:11]=1)[C:8]#[N:9])([CH3:18])[CH3:17]参加物
3
実験手順
Substitution of an equivalent quantity of the preceding acetonitrile for α-[2-(diisopropylamino)ethyl]-α-phenylacetonitrile called for in Example 2, Method B and substantial repetition of the procedure detailed in that example, affords α,α-bis[2-(diisopropylamino)ethyl]-α-(2-pyridyl)acetonitrile, as an oil boiling at about 155°-160° C. at 0.3 mm. pressure.
出典と根拠
- ORDレコード
- ord-a6e69cff00264bffadfcde88ffed5e31
- 出典データセット
- uspto-grants-1979_05
- 特許番号
- US04153797
関連ノート
読み込み中…