Vanillin → Ferulic Acid

HRID 262353

反応式

HRID 262353 の反応式
[CH3:1][O:2][C:3]1[CH:8]=[C:7]([CH:9]=O)[CH:6]=[CH:5][C:4]=1[OH:11].[C:12]([O:15]C(=O)C)(=[O:14])[CH3:13]>>[C:12]([OH:15])(=[O:14])/[CH:13]=[CH:9]/[C:7]1[CH:6]=[CH:5][C:4]([OH:11])=[C:3]([O:2][CH3:1])[CH:8]=1

参加物

3

実験手順

Vaniline is reacted according to Perkin's reaction with acetic anhydride to form ferulic acid which is then decarbonized by heating to prepare 3-methoxy-4-hydroxystyrene. This compound is then acetylated with acetic anhydride, polymerized and then hydrolyzed to obtain 3-methoxy-4-hydroxystyrene polymer. ##STR4## wherein n stands for a positive number corresponding to the number of monomeric units in the polymer.

出典と根拠

ORDレコード
ord-cc7e7a77387148e2acc9db9b074a2e1c
出典データセット
uspto-grants-1979_05
特許番号
US04154653

関連ノート

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