化工社化工社 化学情報印刷レポート · 研究参考用
Hydrochloric Acid → rac-(1R,2R)-2-(dimethylamino)cyclohexan-1-ol
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Hydrochloric Acid | HCID 313 | — |
| 反応物 | Dimethylamine | HCID 674 | — |
| 反応物 | Cyclohexene oxide | HCID 9246 | — |
| 溶媒 | Benzene | HCID 241 | — |
| 生成物 | rac-(1R,2R)-2-(dimethylamino)cyclohexan-1-ol | HCID 15560793 | — |
反応手順
This compound was previously prepared from cyclohexene oxide and dimethylamine in benzene at room temperature for 14 days in 95% yield, b.p. 90° (20 mm): J. Chem. Soc., 4835 (1965); or in autoclave: C. A. 67, 63899 d, Rocz. Chem. 41, 541 (1967) b.p. 88° (14 mm); also Bull. Soc. Chim. France, 850 (1947): hydrochloride and resolution reported.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04148914 |
| 出典データセット | uspto-grants-1979_04 |
| ORD ID | ord-89c4a44e39b04448b933484d36cfabda |
| 出典メモ | uspto-grants-1979_04 |