反応式
[C:1]([OH:6])(=[S:5])[CH:2](C)O.[F:7][C:8]([F:15])([F:14])[C:9](=[CH2:13])[C:10]([OH:12])=[O:11]>>[C:1]([S:5][CH2:13][CH:9]([C:8]([F:15])([F:14])[F:7])[C:10]([OH:12])=[O:11])(=[O:6])[CH3:2]参加物
3
実験手順
A mixture of thiolactic acid (50 g.) and 2-(trifluoromethyl)acrylic acid [M. W. Buxton, et al., J. Chem. Soc., 366 (1954)] (66 g.) is heated on the steam bath for one hour and then stored at room temperature for eighteen hours. The reaction mixture is distilled in vacuo to give 3-acetylthio-2-trifluoromethylpropanoic acid.
後処理
- temperatureis heated on the steam bath for one hour
- waitstored at room temperature for eighteen hours
- distillationThe reaction mixture is distilled in vacuo
出典と根拠
- ORDレコード
- ord-7c2fa40d98714ddea863ba2fc0ff96a4
- 出典データセット
- uspto-grants-1979_05
- 特許番号
- US04154935
関連ノート
読み込み中…