1,1-Dimethylhydrazine → 1,1-Dimethyl-2-(3,4-dichloro-6-nitrophenyl)hydrazine

反応式

[Cl:1][C:2]1[CH:7]=[C:6]([N+:8]([O-:10])=[O:9])[C:5](Cl)=[CH:4][C:3]=1[Cl:12].[CH3:13][N:14]([CH3:16])[NH2:15]>>[CH3:13][N:14]([CH3:16])[NH:15][C:5]1[C:6]([N+:8]([O-:10])=[O:9])=[CH:7][C:2]([Cl:1])=[C:3]([Cl:12])[CH:4]=1

参加物

反応物 2

HCID 59761,1-Dimethylhydrazine

HCID 69832,4,5-Trichloronitrobenzene

生成物 1

HCID 131012921,1-Dimethyl-2-(3,4-dichloro-6-nitrophenyl)hydrazine

実験手順

Reaction of 1,2,4-trichloro-5-nitrobenzene with 1,1-dimethylhydrazine as described in Example I gave the desired product, m.p. 138°-143° C.

出典と根拠

ORDレコード: ord-2d47f7269e794370b1dedbb4c3682f4d
出典データセット: uspto-grants-1979_05
DOI: 10.6084/m9.figshare.5104873.v1
特許番号: US04156083

反応ノート

読み込み中…