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2,5-Dimethyl-1H-indole → 3-(4-Chloro-3-sulfamoylbenzoyl)-2,5-dimethylindole
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 2,5-Dimethyl-1H-indole | HCID 70965 | — |
| 反応物 | 3-(Aminosulfonyl)-4-chlorobenzoyl chloride | HCID 3017979 | — |
| 反応物 | Aluminum(III) Chloride | HCID 6451240 | — |
| 溶媒 | 1,1-Dichloroethane | HCID 6365 | — |
| 生成物 | 3-(4-Chloro-3-sulfamoylbenzoyl)-2,5-dimethylindole | HCID 21316609 | — |
反応手順
is obtained as described in Example 10 (a) from 10 g 4-chloro-3-sulfamoylbenzoyl chloride and 7.8 g 2,5-dimethylindole in dichloro-ethane in the presence of 12 g aluminum chloride. M.p. 248°-250° C.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04156732 |
| 出典データセット | uspto-grants-1979_05 |
| ORD ID | ord-3d6c2c9aa8a744cf8b6d9ed661a2a213 |
| 出典メモ | uspto-grants-1979_05 |