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3-Methylbenzo[b]thiophene → 2-(4-Chloro-3-sulfamoylbenzoyl)-3-methyl-benzo[b]thiophene
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 3-Methylbenzo[b]thiophene | HCID 73817 | — |
| 反応物 | 3-(Aminosulfonyl)-4-chlorobenzoyl chloride | HCID 3017979 | — |
| 反応物 | Aluminum(III) Chloride | HCID 6451240 | — |
| 溶媒 | Chlorobenzene | HCID 7964 | — |
| 生成物 | 2-(4-Chloro-3-sulfamoylbenzoyl)-3-methyl-benzo[b]thiophene | HCID 21316639 | — |
反応手順
is obtained as described in Example 1 from 2.5 g 4-chloro-3-sulfamoylbenzoyl chloride, 1.6 g 3-methylbenzo[b]thiophene and 3 g aluminum chloride in 50 ml chlorobenzene. Colorless crystals, m.p. 210° C.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04156732 |
| 出典データセット | uspto-grants-1979_05 |
| ORD ID | ord-c924855fb6344a32ab7dcacaf651a47f |
| 出典メモ | uspto-grants-1979_05 |